Wednesday, June 27, 2012
EI2302 ANALYTICAL INSTRUMENTS Syllabus - EIE 5th Semester - Anna University
EI2302 ANALYTICAL INSTRUMENTS LT P C
3 0 0 3
AIM
The course is designed to equip the students with an adequate knowledge of a number
of
analytical tools which are useful
for clinical analysis in hospitals, drugs and pharmaceutical laboratories and above all for
environmental
Pollution Monitoring.
OBJECTIVES
i. To provide various techniques and methods of analysis which occur
in
the various regions of
the spectrum. These are the powerful tools used in Clinical and Research laboratories.
ii. To give unique methods of separation of closely similar materials, the most powerful being
gas
chromatography.
iii. To study important methods of analysis of industrial gases. Awareness and control of
pollution in the environment is of vital
importance.
iv. To bring out the latest ideas on ion-selective electrodes as well as biosensors which have potential applications in medical field, food and beverage industries.
v. To provide the important electromagnetic resonance and microscopic methods of analysis.
Further they are both sensitive and specific and often are characterized by good accuracy.
NMR
& ESR and microscopic techniques are useful in structure determination.
UNIT I
COLORIMETRY AND
SPECTROPHOTOMETRY
9
Special methods of analysis – Beer-Lambert law
– Colorimeters – UV-Visible spectrophotometers –
Single and double beam instruments – Sources and detectors – IR Spectrophotometers – Types – Attenuated total reflectance flame photometers
– Atomic
absorption spectrophotometers – Sources
and detectors
– FTIR spectrophotometers – Flame emission photometers – Fluorescence spectrophotometer
UNIT II CHROMATOGRAPHY
9
Different techniques
– Gas chromatography – Detectors – Liquid chromatographs – Applications – High-pressure liquid chromatographs – Applications.
UNIT III
INDUSTRIAL GAS ANALYZERS AND
POLLUTION MONITORING
INSTRUMENTS 9
Types of gas analyzers – Oxygen, NO2 and H2S
types,
IR analyzers, thermal conductivity analyzers, analysis based on ionization of gases. Air
pollution due to carbon monoxide,
hydrocarbons, nitrogen oxides, sulphur
dioxide estimation -
Dust and smoke measurements.
UNIT IV pH METERS AND DISSOLVED
COMPONENT ANALYZERS 9
Principle of
pH measurement,
glass electrodes,
hydrogen
electrodes,
reference electrodes, selective ion electrodes, ammonia electrodes,
cyclic voltametry, biosensors, dissolved oxygen
analyzer – Sodium analyzer
– Silicon analyzer.
UNIT V ELECTRO MAGNETIC RESONANCE AND MICROSCOPIC TECHNIQUES
9
NMR – Basic principles – NMR spectrometer - Applications. Electron spin Resonance spectroscopy
– Basic principles, Instrumentation and applications. Scanning Electron Microscope (SEM), -
Basic
principles, Instrumentation and applications. Transmission Electron Microscope (TEM) – Basic principles – Instrumentation and applications.
Mass spectrometers – Different types – Applications.
TOTAL : 45 PERIODS
TEXT BOOKS:
1. G.W. Ewing, ‘Instrumental Methods of Analysis’, McGraw Hill, 1992.
2. R.K.Jain, Mechanical
and Industrial Measurements, Khanna Publishers, New
Delhi, 1999
3. H.H. Willard, L.L.
Merritt,
J.A. Dean, F.A. Settle,
‘Instrumental Methods of Analysis’, CBS
publishing & distribution, 1995.
REFERENCES:
1. Robert D. Braun, ‘Introduction to Instrumental Analysis’, McGraw
Hill, Singapore, 1987.
2. R.S. Khandpur, ‘Handbook of Analytical Instruments’, Tata McGraw Hill publishing Co. Ltd.,
2003.
3. Liptak, B.G, Process Measurement and
Analysis, Chilton Book Company, 1995
By Vinoth
Subscribe to:
Post Comments (Atom)
0 Responses to “EI2302 ANALYTICAL INSTRUMENTS Syllabus - EIE 5th Semester - Anna University”
Post a Comment